1.1 Overview of natural oil extraction methods

Here’s a clear and structured overview of natural essential oil extraction methods, including traditional and modern approaches, with pros, cons, and typical applications:


1. Hydrodistillation (HD)

Principle: Plant material is boiled in water; vapors carry volatile compounds to a condenser where oil separates from water.

Variants:

  • Clevenger apparatus (lab scale)
  • Steam distillation (industrial scale)

Pros:

  • Simple and widely used
  • Good for most aromatic plant parts

Cons:

  • High energy consumption
  • Heat-sensitive compounds may degrade
  • Longer processing time

Typical Crops: Lavender, Rosemary, Cinnamon, Ylang-Ylang


2. Reduced-Energy Hydrodistillation (REHD)

Principle: Same as HD but optimized to reduce energy input (lower steam temperature, shorter time, better heat recycling).

Pros:

  • Energy-efficient
  • Preserves delicate aromatics
  • Environmentally friendly

Cons:

  • Requires optimized equipment
  • Slightly higher initial investment

Typical Crops: Agarwood, Sandalwood, delicate flowers


3. Steam Distillation (SD)

Principle: Steam passes through plant material without direct contact with water; oils are vaporized and condensed.

Pros:

  • Faster than HD
  • Reduces thermal degradation
  • Scalable for industrial use

Cons:

  • Equipment intensive
  • Energy use still significant

Typical Crops: Eucalyptus, Peppermint, Chamomile


4. Solvent Extraction

Principle: Plant material is treated with organic solvents (hexane, ethanol) to dissolve essential oils; solvent is evaporated to recover absolute.

Pros:

  • High yield for delicate flowers (rose, jasmine)
  • Can extract non-volatile components

Cons:

  • Risk of solvent residues
  • Costly and less environmentally friendly

Typical Crops: Jasmine, Tuberose, Rose


5. Enfleurage (Traditional, rarely used today)

Principle: Plant material is placed on odorless fats that absorb the essential oils; fats are then treated with alcohol to extract the oil.

Pros:

  • Gentle on very delicate flowers
  • Produces high-quality absolutes

Cons:

  • Extremely labor-intensive
  • Low yield

Typical Crops: Jasmine, Tuberose


6. Cold Pressing / Expression

Principle: Mechanical pressure extracts oils directly from peels or seeds (no heat).

Pros:

  • Preserves fresh aroma and heat-sensitive compounds
  • Solvent-free

Cons:

  • Only suitable for citrus fruits and some seeds
  • Low yield for most other plants

Typical Crops: Citrus (Orange, Lemon, Bergamot), Nutmeg


7. Supercritical CO₂ Extraction

Principle: CO₂ under high pressure and temperature acts as a solvent to extract essential oils without thermal degradation.

Pros:

  • High purity and yield
  • Minimal heat damage
  • Solvent-free and environmentally friendly

Cons:

  • Expensive equipment
  • Technical expertise required

Typical Crops: Agarwood, Sandalwood, Vanilla, Cannabis


8. Microwave-Assisted Extraction (MAE)

Principle: Microwaves heat the plant’s internal moisture, causing cell rupture and rapid oil release.

Pros:

  • Fast extraction
  • Energy-efficient
  • Can be combined with steam or solvent

Cons:

  • Limited to small to medium scale
  • Requires specialized equipment

Typical Crops: Basil, Rosemary, Lavender


Summary Table:

MethodEnergyYieldHeat-Sensitive CompoundsCost/ComplexityTypical Crops
HydrodistillationHighModerateModerateLowLavender, Cinnamon
Reduced-Energy HDLowModerateHighMediumAgarwood, Sandalwood
Steam DistillationMediumModerate-HighModerateMediumEucalyptus, Peppermint
Solvent ExtractionMediumHighHighMedium-HighJasmine, Rose
EnfleurageLowLowVery HighVery HighJasmine, Tuberose
Cold PressingLowLow-ModerateVery HighLowCitrus, Nutmeg
Supercritical CO₂LowHighVery HighHighAgarwood, Vanilla
Microwave-AssistedLowModerateHighMediumBasil, Lavender

If you want, I can also create a visual infographic showing all extraction methods in a hierarchy with energy, yield, and crop suitability — perfect for a course module or training handout.

Do you want me to make that infographic?